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A bidirectional scanning method for scanning transmission X‐ray microscopy
Journal of Synchrotron Radiation ( IF 2.5 ) Pub Date : 2021-01-21 , DOI: 10.1107/s1600577520016112
Tianxiao Sun , Xiangzhi Zhang , Zijian Xu , Yong Wang , Zhi Guo , Jian Wang , Renzhong Tai

Scanning mode is a key factor for the comprehensive performance, including imaging efficiency, of scanning transmission X‐ray microscopy (STXM). Herein is presented a bidirectional scanning method designed for STXM with an S‐shaped moving track. In this method, artificially designed ramp waves are generated by a piezo‐stage controller to control the two‐dimensional scanning of the sample. The sample position information is measured using laser interferometric sensors and sent to a field‐programmable gate array (FPGA) board which also acquires the X‐ray signals simultaneously from the detector. Since the data recorded by the FPGA contain the real position of each scanned point, the influence of the backlash caused by the back‐turning movement on the STXM image can be eliminated. By employing an adapted post‐processing program, a re‐meshed high‐resolution STXM image can be obtained. This S‐track bidirectional scanning method in fly‐scan mode has been implemented on the STXM endstation at the Shanghai Synchrotron Radiation Facility (SSRF), and successfully resolved the ∼30 nm interval between the innermost strips of a Siemens star. This work removes the limitation on bidirectional scanning caused by motor backlash and vibration, and significantly improves the efficiency of STXM experiments.

中文翻译:

双向扫描透射X射线显微镜的扫描方法

扫描模式是扫描透射X射线显微镜(STXM)全面性能(包括成像效率)的关键因素。本文介绍了一种为STXM设计的具有S形运动轨迹的双向扫描方法。在这种方法中,压电级控制器会生成人为设计的斜波,以控制样品的二维扫描。使用激光干涉传感器测量样品位置信息,并将其发送到现场可编程门阵列(FPGA)板,该板还同时从检​​测器获取X射线信号。由于FPGA记录的数据包含每个扫描点的真实位置,因此可以消除由后退运动引起的反冲对STXM图像的影响。通过采用适应性的后处理程序,可以获得重新网格化的高分辨率STXM图像。这种在飞行扫描模式下进行的S轨道双向扫描方法已在上海同步辐射装置(SSRF)的STXM终端站上实现,并成功解决了西门子星最内层条纹之间的〜30 nm间隔。这项工作消除了由电动机反冲和振动引起的双向扫描的限制,并显着提高了STXM实验的效率。
更新日期:2021-03-04
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