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Functionalization of kaolin clay with silver nanoparticles by Murraya koenigii fruit extract-mediated bioreduction process for antimicrobial applications
Journal of the Australian Ceramic Society ( IF 1.9 ) Pub Date : 2021-01-07 , DOI: 10.1007/s41779-020-00545-2
M. Hariram , V. Ganesan , S. Muthuramkumar , S. Vivekanandhan

The emergence of multidrug-resistant microbes and newly outbreaking diseases are one of the major threats before mankind. This paves the way for researchers to explore new antimicrobial agents that possess common day-to-day applications. In this concern, we have fabricated the antimicrobial Ag-kaolin functional nanostructures by simple and sustainable protocol employing Murraya koenigii fruit extract. UV-visible spectra (UV-Vis) of the Ag-kaolin exhibit absorption peak at 430 nm which corresponds to the characteristic surface plasmon resonance of Ag nanoparticles. X-ray diffraction pattern (XRD) shows the diffraction peak at 37.6° confirms their face-centred cubic nature with (111) plane. Furthermore, the formation of Ag-kaolin functional nanostructures was confirmed through a scanning electron microscope (SEM) and energy-dispersive X-ray spectrum (EDX) analysis. The transmission electron microscopic (TEM) studies reveal the effective formation of quasi-spherical monodispersed Ag nanoparticles having 20–30-nm diameters on the kaolin clay. The bio-synthesized Ag-kaolin nanostructures showed excellent antimicrobial activity against pathogenic gram-positive (Staphylococcus aureus, Bacillus subtilis) and gram-negative (Escherichia coli) bacteria respectively with the inhibition zones of 26 mm, 25 mm and 30 mm.



中文翻译:

Murraya koenigii水果提取物介导的生物还原工艺将高岭土与银纳米颗粒官能化,用于抗菌应用

耐多药微生物的出现和新近爆发的疾病是人类面临的主要威胁之一。这为研究人员探索具有常见日常应用的新型抗菌剂铺平了道路。考虑到这一点,我们通过使用Murraya koenigii的简单且可持续的方案制备了抗菌型Ag-高岭土功能纳米结构水果提取物。Ag-高岭土的UV-可见光谱(UV-Vis)在430nm处显示吸收峰,其对应于Ag纳米颗粒的特征性表面等离子体共振。X射线衍射图谱(XRD)显示37.6°处的衍射峰证实了它们的面心立方性质为(111)平面。此外,通过扫描电子显微镜(SEM)和能量色散X射线光谱(EDX)分析证实了Ag-高岭土功能纳米结构的形成。透射电子显微镜(TEM)研究表明,高岭土上有效形成了直径为20–30 nm的准球形单分散Ag纳米颗粒。生物合成的银高岭土纳米结构对病原性革兰氏阳性金黄色葡萄球菌枯草芽孢杆菌Bacillus subtilis)和革兰氏阴性(Escherichia coli)细菌分别具有26 mm,25 mm和30 mm的抑制区。

更新日期:2021-01-07
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