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Compressed fluids extraction methods, yields, antioxidant activities, total phenolics and flavonoids content for Brazilian Mantiqueira hops
The Journal of Supercritical Fluids ( IF 3.9 ) Pub Date : 2020-12-29 , DOI: 10.1016/j.supflu.2020.105155
Bruno Aguilar Veiga , Fabiane Hamerski , Mathias Porsmose Clausen , Massimiliano Errico , Agnes de Paula Scheer , Marcos Lúcio Corazza

This study compares the yields of different extractions methods for a Brazilian variety of Humulus lupulus using scCO2, scCO2 + ethanol, scCO2 + ethyl acetate, and compressed propane. Extracts were characterized by total phenolics content (TPC), total flavonoid content (TFC), and antioxidant activity (AA). The extraction yields were from 2.7 to 10.1 wt% when using compressed propane at 20 °C and 10 MPa and scCO2 + ethyl acetate at 80 °C and 25 MPa, respectively. Furthermore, the effect of adding ethyl acetate as a cosolvent in a semi-batch process over the extraction time and extracts properties were evaluated in comparison to the extracts obtained using scCO2, scCO2 + ethanol, and compressed propane. The results indicate that ethyl acetate increases the extraction yield and produces samples with higher TPC, TFC, and AA values comparing to scCO2 + ethanol and similar values compared to pure scCO2.



中文翻译:

巴西Mantiqueira啤酒花的压缩液提取方法,产率,抗氧化活性,总酚和类黄酮含量

这项研究比较了使用scCO 2,scCO 2 +乙醇,scCO 2 +乙酸乙酯和压缩丙烷对巴西variety的不同提取方法的产量。提取物的特征在于总酚含量(TPC),总黄酮含量(TFC)和抗氧化活性(AA)。当分别使用20°C和10 MPa的压缩丙烷和80°C和25 MPa的scCO 2 +乙酸乙酯时,萃取产率为2.7至10.1 wt%。此外,与使用scCO 2,scCO 2获得的萃取物相比,评估了在半间歇过程中在萃取过程中加入乙酸乙酯作为助溶剂的效果和萃取物性质。+乙醇和压缩丙烷。结果表明,与scCO 2 +乙醇相比,乙酸乙酯可提高提取产率,并产生具有更高TPC,TFC和AA值的样品,而与纯scCO 2相比,乙酸乙酯的值相似。

更新日期:2021-01-06
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