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New bisphosphonium salt containing a 1,4-dihydroxynaphthalene moiety: molecular and supramolecular structure
Russian Chemical Bulletin ( IF 1.7 ) Pub Date : 2020-11-01 , DOI: 10.1007/s11172-020-3012-3
N. R. Khasiyatullina , A. T. Gubaidullin , A. M. Shinkareva , D. R. Islamov , V. F. Mironov

Bisphosphonium salt containing a 1,4-dihydroxynaphthyl-substituted moiety was synthesized in high yield by the reaction of 2-methyl-1,4-naphthoquinone with three equivalents of triphenylphosphine and hydrogen bromide. The structure of the synthesized bisphosphonium salt was determined by NMR spectroscopy and X-ray diffraction.

中文翻译:

含有 1,4-二羟基萘部分的新型双鏻盐:分子和超分子结构

通过 2-甲基-1,4-萘醌与三当量的三苯基膦和溴化氢反应,以高收率合成了含有 1,4-二羟基萘基取代部分的双鏻盐。合成的双鏻盐的结构通过核磁共振光谱和 X 射线衍射确定。
更新日期:2020-11-01
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