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In-situ ion irradiation induced grain growth in nanocrystalline ceria
Journal of Nuclear Materials ( IF 3.1 ) Pub Date : 2020-11-30 , DOI: 10.1016/j.jnucmat.2020.152688
C.J. Ulmer , W-Y. Chen , D.E. Wolfe , A.T. Motta

Irradiation grain growth of CeO2 was studied using in-situ ion irradiation with transmission electron microscopy (TEM). Thin films of ceria were produced by electron beam physical vapor deposition (EB-PVD) and then irradiated at the Intermediate Voltage Electron Microscope (IVEM) with 1 MeV Kr2+ ions at temperatures of 400°C, 600°C, and 800°C. During irradiation at the elevated temperatures, the CeO2 phase remained stable and its grains grew with irradiation. Grain growth was only weakly dependent on irradiation temperature between 400°C and 800°C. The grain growth kinetics were evaluated by a thermal spike model that was used to calculate the activation energy for grain growth.



中文翻译:

原位离子辐照诱导纳米晶二氧化铈晶粒长大

使用透射电子显微镜(TEM)进行原位离子辐照研究了CeO 2辐照晶粒的生长。通过电子束物理气相沉积(EB-PVD)制备二氧化铈薄膜,然后在400°C,600°C和800°C的温度下,用1 MeV Kr 2+离子在中压电子显微镜(IVEM)上辐照。C。在高温下照射期间,CeO 2相保持稳定并且其晶粒随照射而生长。晶粒生长仅微弱地依赖于400°C至800°C之间的辐照温度。通过热峰值模型评估了晶粒生长动力学,该模型用于计算晶粒生长的活化能。

更新日期:2020-12-17
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