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Manufacturing and Testing of an In Situ Stretching Sample Environment Equipment for Neutron Scattering Experiments
Science and Technology of Nuclear Installations ( IF 1.1 ) Pub Date : 2020-11-27 , DOI: 10.1155/2020/8867688
Haibin Chen 1, 2, 3 , Rongyong Li 1, 2, 3 , Yu Liu 2, 3, 4
Affiliation  

Neutron scattering technology is one of the most promising ways to observe microstructures of different materials. As a powerful microstructure characterization technology, neutron scattering is widely used in many disciplines. With the help of sample environment equipment, the microstructure detection for materials in various application scenarios can be further realized. In order to detect the microstructure changes of materials under different tensile conditions, an in situ stretching sample environment equipment for neutron scattering experiments was designed and manufactured. Stretching force holding test, sample breaking test, and vacuum maintaining test were carried out. In those tests, a tensile force holding test with no less than 5 hours, a breaking test with a screw bolt as the sample, and a vacuum leakage rate test with no less than 5 hours were obtained, respectively. Through analyzing values obtained, it is shown that the developed prototype of the sample environment equipment is able to meet the experiment requirements. The present prototype provides a reference for further development of sample environment equipment for different application scenarios in neutron scattering experiment.

中文翻译:

用于中子散射实验的原位拉伸样品环境设备的制造和测试

中子散射技术是观察不同材料微观结构的最有前途的方法之一。中子散射作为一种强大的微结构表征技术,已在许多学科中得到广泛应用。借助样品环境设备,可以进一步实现各种应用场景下材料的微观结构检测。为了检测不同拉伸条件下材料的微观结构变化,设计并制造了用于中子散射实验的原位拉伸样品环境设备。进行拉伸力保持测试,样品断裂测试和真空保持测试。在那些测试中,不小于5小时的拉伸力保持测试,以螺栓为样本的断裂测试,获得了不少于5小时的真空泄漏率测试。通过分析获得的值,表明所开发的样品环境设备原型能够满足实验要求。本原型为中子散射实验中不同应用场景的样品环境设备的进一步开发提供了参考。
更新日期:2020-11-27
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