Superfine pulverisation (SFP) pretreatment of Lycium barbarum L. leaves was performed to obtain highly crystalline cellulose. Compared with other common pulverisation methods, SFP enhanced cellulosic crystallinity by 18.3 % and 8.4 %, with and without post-acid treatments, respectively. XRD and solid-state NMR analyses showed that SFP facilitated the exposure of amorphous substances (i.e., hemicellulose and lignin) to NaOH and H₂O₂. Large amounts of silicon (5.5 %) and aluminium (2.1 %) were found to incorporate into the crystalline regions of SFP-produced cellulose. Further FTIR and thermogravimetric analyses revealed that SFP-produced cellulose contained large amounts of hydroxyl groups, affecting the cellulosic crystallinity and thermal stability. These findings demonstrate the potential for SFP to serve as a green technology for production of highly crystalline and mineral-rich cellulose.

进行枸杞叶片的超细粉碎（SFP）预处理以获得高度结晶的纤维素。与其他常见的粉碎方法相比，SFP经过和不经过后酸处理后，纤维素的结晶度分别提高了18.3％和8.4％。XRD和固态NMR分析表明，SFP促进了无定形物质（即半纤维素和木质素）暴露于NaOH和H ₂ O ₂。发现大量硅（5.5％）和铝（2.1％）掺入SFP生产的纤维素的结晶区域中。进一步的FTIR和热重分析表明，SFP生产的纤维素含有大量羟基，影响纤维素的结晶度和热稳定性。这些发现表明，SFP有潜力用作生产高度结晶和富含矿物质的纤维素的绿色技术。