We describe a simple apparatus that enables the vacuum distillation of ~0.2 mL of air- and water-sensitive, high-boiling liquids. The apparatus should be useful in teaching laboratories, and also to practicing chemists.

中文翻译：

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用于高沸点，对空气和热敏感液体的微型真空蒸馏设备

我们描述了一种简单的装置，该装置能够真空蒸馏约0.2 mL的对空气和水敏感的高沸点液体。该设备应在实验室教学和化学工作者实践中有用。