Mesoporous PbTiO₃ nanosheets were synthesized by a one-step sol-gel process employing the F127 surfactant as a structure directing agent. Different percentages of platinum nanoparticles (0.2–0.8 wt%) were deposited onto mesoporous PbTiO₃ nanosheets surface employing a photoassisted deposition method. TEM images of Pt@PbTiO₃ mesoporous nanocomposites show the close proximity of lattice fringes 0.220 nm of metallic platinum (111) and the 0.284 nm lattice layout of the PbTiO₃ (101). The synthesized Pt@PbTiO₃ mesoporous composites were tested in the presence of glycerol employing visible light derived photocatalytic water splitting reaction. The H₂ evolution rate with the use of 0.6 wt% Pt@PbTiO₃ reached 3564 μmol/g, which is 85 times higher than the rate when pure mesoporous PbTiO₃ was used. The H₂ evolution rate when using PbTiO₃ was 42 μmol g⁻¹ h⁻¹, which was enhanced to 3564 μmol g⁻¹ h⁻¹ upon the use of 0.6 wt% Pt@PbTiO₃. Pt@PbTiO₃ nanocomposites exhibit excellent photocatalytic activity with outstanding stability and enhanced possibility of reuse with a potential to be used in environmental and energy applications.

介孔的PbTiO ₃纳米片是采用F127表面活性剂作为结构导向剂，通过一步溶胶-凝胶法合成的。采用光辅助沉积方法，将不同百分比的铂纳米颗粒（0.2–0.8 wt％）沉积在中孔PbTiO ₃纳米片表面上。Pt @ PbTiO ₃介孔纳米复合材料的TEM图像显示，金属铂（111）的晶格条纹为0.220 nm，PbTiO ₃（101）的晶格布局为0.284 nm 。在可见光衍生的光催化水分解反应条件下，在甘油存在下测试了合成的Pt @ PbTiO ₃介孔复合材料。H ₂使用0.6wt％的Pt @ PbTiO _3的析出速率达到3564μmol/ g，这是使用纯中孔PbTiO ₃的速率的85倍。为H ₂使用的PbTiO时释放速率₃为42微摩尔克^-1  ħ ^-1，这是增强的3564微摩尔克^-1  ħ ^-1于使用0.6重量％Pt的PbTiO @的₃。Pt @ PbTiO ₃纳米复合材料具有出色的光催化活性，具有出色的稳定性和增强的再利用可能性，可用于环境和能源应用。