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Synthesis of New Chromene-Containing Pyrrolofullerenes
Russian Journal of General Chemistry ( IF 0.9 ) Pub Date : 2020-08-10 , DOI: 10.1134/s1070363220070269
O. A. Nurkenov , S. D. Fazylov , A. E. Arinova , T. M. Seilkhanov , M. K. Ibraev , E. M. Tazhbaev

Abstract

Three-component condensation of substituted 4-oxochromene-3-carbaldehydes with sarcosine and fullerene C60 afforded 2′-(4-oxochromen-3-yl)-1′-methyl-2′,5′-dihydro-1′H-pyrrolo[3′,4′:1,9](C60-Ih)[5,6]fullerenes. The structure of the synthesized compounds was studied by 1H and 13C NMR spectroscopy, including 1H–1H COSY and 1H–13C HMQC experiments.


中文翻译:

新型含Chromene的吡咯并富勒烯的合成

摘要

取代的4- oxochromene -3- carbaldehydes用肌氨酸和富勒烯C的三组分缩合60,得到2' - (4-氧代苯并吡喃-3-基)-1'-甲基-2',5'-二氢-1' ħ -吡咯并[3',4':1,9](C 60 - I h)[5,6]富勒烯。通过1 H和13 C NMR光谱研究了合成化合物的结构,包括1 H– 1 H COZY和1 H– 13 C HMQC实验。
更新日期:2020-08-10
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