Key comparison study—organic solvent calibration solution—gravimetric preparation and value assignment of trans-zearalenone (trans-ZEN) in acetonitrile (ACN),Metrologia

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Key comparison study—organic solvent calibration solution—gravimetric preparation and value assignment of trans-zearalenone (trans-ZEN) in acetonitrile (ACN)
Metrologia ( IF 2.4 ) Pub Date : 2020-08-03 , DOI: 10.1088/0026-1394/57/1a/08019
R D Josephs ₁ , A Daireaux ₁ , M Bedu ₁ , Xiuqin Li _{1,

2} , Xiaomin Li _{1,

2} , Z Guo _{1,

2} , T Choteau ₁ , G Martos ₁ , S Westwood ₁ , R I Wielgosz ₁ , H Li ₂ , M Simón ₃ , E C P do Rego ₄ , B C Garrido ₄ , R Leal ₄ , L Carvalho ₄ , E Guimarães ₄ , A Bahadoor ₅ , J Bates ₅ , J E Melanson ₅ , P Giannikopoulou ₆ , C Alexopoulos ₆ , E Kakoulides ₆ , I Mugenya ₇ , D Prevoo-Franzsen ₈ , M Fernandes-Whaley ₈ , S Marbumrung ₉ , M Bilsel ₁₀ , B Binici ₁₀ , T Gokcen ₁₀

Affiliation

The CCQM-K154.a and subsequent CCQM-K154.a.1 comparisons were coordinated by the the Bureau International des Poids et Mesures (BIPM) and the Chinese National Institute of Metrology (NIM) on behalf of the Organic Analysis Working Group (OAWG) of the Comité Consultatif pour la Quantité de Matière (CCQM) for National Measurement Institutes (NMIs) and Designated Institutes (DIs) which provide measurement services in organic analysis under the 'Comité International des Poids et Mesures' Mutual Recognition Arrangement (CIPM MRA) and/or have participated in the BIPM's Mycotoxin Metrology Capacity Building and Knowledge Transfer (MMCBKT) project as part of its "Metrology for Safe Food and Feed in Developing Economies" Capacity Building Programme. Gravimetrically-prepared solutions having an assigned mass fraction of specified organic analytes are routinely used to calibrate measurement processes for the quantification of the same analytes in matrix samples. Appropriate assignmen...

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