Metallurgical and Materials Transactions A ( IF 2.8 ) Pub Date : 2020-07-07 , DOI: 10.1007/s11661-020-05894-y Marcin Nabiałek , Bartłomiej Jeż , Katarzyna Błoch
This study aims to determine the effect of addition of a small quantity of Si on the formation of nanocrystalline structure in rapidly cooled Fe-Co-B alloys. As part of the work, the following alloys were produced using a method involving the forcing of each respective liquid alloy into a copper mold: Fe65Co11−xB20SixZr2Hf2 (where: x = 0; 0.25; 0.5; 0.75; 1). Analysis of recorded X-ray diffraction patterns confirmed that a nanocrystalline structure was obtained in the alloys. The intensity of the diffraction reflections was found to change with changing Si content. The Fe23B6 crystalline phase was present in the volume of each alloy. This phase has soft magnetic properties. The presence of the Fe23B6 phase was confirmed by measurements of the magnetic polarization of saturation as a function of temperature.
中文翻译:
硅含量对Fe 65 Co 11-x B 20 Si x Zr 2 Hf 2块状非晶态合金中Fe 23 B 6亚稳相形成的影响
这项研究旨在确定在快速冷却的Fe-Co-B合金中添加少量Si对纳米晶体结构形成的影响。作为工作的一部分,使用涉及将每种液态合金强制压入铜模的方法生产以下合金:Fe 65 Co 11- x B 20 Si x Zr 2 Hf 2(其中:x = 0; 0.25; 0.5; 0.75; 1)。对记录的X射线衍射图谱的分析证实了在合金中获得了纳米晶体结构。发现衍射反射的强度随Si含量的变化而变化。铁23 B 6每种合金的体积中都存在结晶相。该相具有软磁特性。Fe 23 B 6相的存在通过测量饱和磁极化强度随温度的变化来确定。