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INVESTIGATION OF POROUS ANODIC FILM FORMATION ON AA1050 BY ELECTROCHEMICAL IMPEDANCE SPECTROSCOPY
Surface Review and Letters ( IF 1.1 ) Pub Date : 2019-11-13 , DOI: 10.1142/s0218625x19501865
M. DANIŞMAN 1 , M. KOCABAŞ 2 , M. CURIONI 3 , N. CANSEVER 4
Affiliation  

In this study, the formation of porous Al2O3 on commercial 1050 aluminium alloy (AA1050) in 2[Formula: see text]M sulfuric acid (H2SO4) electrolyte was investigated. Anodization was performed at 12[Formula: see text]V and 15[Formula: see text]V specimens for a charge density of 757[Formula: see text]mC/cm2 and 3231[Formula: see text]mC/cm2. The resulting oxides were analyzed using scanning electron microscopy (SEM). According to analysis, a hexagonal oxide formation containing more than one nano pore was observed on the surface of the specimen. The structural properties of the porous oxide film were analyzed with electrochemical impedance spectroscopy (EIS) analysis and film-related features such as thickness of the porous and the barrier layer were obtained.

中文翻译:

电化学阻抗谱法研究 AA1050 上多孔阳极薄膜的形成

在本研究中,多孔铝的形成23对商用1050铝合金(AA1050)2[配方:见正文]M硫酸(H2所以4) 对电解质进行了研究。阳极氧化在 12[公式:见正文]V 和 15[公式:见正文]V 试样上进行,电荷密度为 757[公式:见正文]mC/cm2和3231【公式:见正文】mC/cm2. 使用扫描电子显微镜 (SEM) 分析所得氧化物。经分析,在试样表面观察到含有多于一个纳米孔的六方氧化物结构。用电化学阻抗谱(EIS)分析法分析了多孔氧化物薄膜的结构特性,并获得了与薄膜相关的特征,例如多孔和阻挡层的厚度。
更新日期:2019-11-13
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