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Preparation and Crystal Growth of Transition Metal Dichalcogenides
Zeitschrift für anorganische und allgemeine Chemie ( IF 1.4 ) Pub Date : 2020-06-17 , DOI: 10.1002/zaac.202000111
Marcus Schmidt 1 , Johannes Gooth 1 , Michael Binnewies 1
Affiliation  

Dichalcogenides are known from almost all transition metals. The representatives of this class of compounds show a number of interesting physical and chemical properties depending on their constituent transition metal and crystal structure, which makes them interesting for basic studies and applications in high‐end electronics, spintronics, optoelectronics, energy storage, flexible electronics, DNA sequencing and personalized medicine to this day. Many of these properties and effects can only be investigated on chemically and crystallographically pure samples ‐ usually on single crystals. The vast majority of these compounds can be crystallized using chemical vapour transport. However crystallization from the melt is also possible in a considerable number of compounds, including the frequently used self‐flux technique. For several compounds the crystallization from different solvents or solvent mixtures by means of solvothermal or hydrothermal synthesis is described.

中文翻译:

过渡金属二硫属元素化物的制备和晶体生长

几乎所有的过渡金属中都已知有硫族元素化物。这类化合物的代表根据其组成的过渡金属和晶体结构显示出许多有趣的物理和化学性质,这使其对于高端电子,自旋电子,光电,储能,柔性电子学的基础研究和应用很有趣。 ,DNA测序和个性化医学到今天。其中许多特性和作用只能在化学和晶体学纯净的样品上进行研究-通常在单晶上进行。这些化合物中的绝大多数可以使用化学气相传输来结晶。但是,在许多化合物中,也可能从熔体中结晶出来,包括经常使用的自通量技术。
更新日期:2020-06-17
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