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Microwave-assisted efficient one-pot synthesis of N 2-(tetrazol-5-yl)-6-aryl/heteroaryl-5,6-dihydro-1,3,5-triazine-2,4-diamines.
Beilstein Journal of Organic Chemistry ( IF 2.7 ) Pub Date : 2020-07-16 , DOI: 10.3762/bjoc.16.142 Moustafa Sherief Moustafa 1 , Ramadan Ahmed Mekheimer 2 , Saleh Mohammed Al-Mousawi 1 , Mohamed Abd-Elmonem 2 , Hesham El-Zorba 3 , Afaf Mohamed Abdel Hameed 2 , Tahany Mahmoud Mohamed 2 , Kamal Usef Sadek 2
Beilstein Journal of Organic Chemistry ( IF 2.7 ) Pub Date : 2020-07-16 , DOI: 10.3762/bjoc.16.142 Moustafa Sherief Moustafa 1 , Ramadan Ahmed Mekheimer 2 , Saleh Mohammed Al-Mousawi 1 , Mohamed Abd-Elmonem 2 , Hesham El-Zorba 3 , Afaf Mohamed Abdel Hameed 2 , Tahany Mahmoud Mohamed 2 , Kamal Usef Sadek 2
Affiliation
An efficient one-pot synthesis of N2-(tetrazol-5-yl)-6-aryl/heteroaryl-1,3,5-triazine-2,4-diamine derivatives was developed by reacting 5-amino-1,2,3,4-tetrazole with aromatic aldehydes and cyanamide in pyridine under controlled microwave heating with high yields. X-ray crystallography confirmed the structure of the obtained products.
中文翻译：
N 2-（四唑-5-基）-6-芳基/杂芳基-5,6-二氢-1,3,5-三嗪-2,4-二胺的微波辅助有效一锅合成。
一种有效的一锅法合成N 2-（四唑-5-基）-6-芳基/杂芳基-1,3,5-三嗪-2,4-二胺衍生物的方法是通过使5-氨基-1,2， 3,4-四唑与芳族醛和氰酰胺的吡啶在可控的微波加热下具有较高的收率。X射线晶体学证实了所得产物的结构。
更新日期：2020-07-16
中文翻译：
N 2-（四唑-5-基）-6-芳基/杂芳基-5,6-二氢-1,3,5-三嗪-2,4-二胺的微波辅助有效一锅合成。
一种有效的一锅法合成N 2-（四唑-5-基）-6-芳基/杂芳基-1,3,5-三嗪-2,4-二胺衍生物的方法是通过使5-氨基-1,2， 3,4-四唑与芳族醛和氰酰胺的吡啶在可控的微波加热下具有较高的收率。X射线晶体学证实了所得产物的结构。
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