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Reduction behaviour of Odisha Sands Complex, India ilmenite-coke composite pellets
Journal of Central South University ( IF 4.4 ) Pub Date : 2020-07-16 , DOI: 10.1007/s11771-020-4399-6
D. Nayak , N. Ray , N. Dash , S. S. Rath , S. K. Biswal

Presently, ilmenite concentrates from Odisha Sands Complex at Chhatrapur, India are utilized to produce TiO2 slag by direct smelting in an electric arc furnace. However, the process involves the consumption of excess electrical energy and difficulty in handling the arc furnace due to frothing effects. A more efficient process of pre-reducing the ilmenite before smelting has been proposed in the present communication. In particular, studies have been undertaken on the reduction process of ilmenite-coke composite pellets. The difference in the reduction behaviour of raw ilmenite and ilmenite-coke composite pellets has been established and compared with that of the pre-oxidized raw pellets. The effects of various processing parameters like temperature, residence time, and reductant percentage on the metallization of composite pellets in a static bed have been investigated. Metallization of about 90% has been achieved at 1250 °C for a reduction period of 360 min with a 4°% coke composition. Furthermore, the reduced pellets have been characterized through chemical analysis, optical microscopy, field emission scanning electron microscopy and X-ray diffraction analysis. The reduction behaviour of composite pellets has also been found better than that of pre-oxidized pellets indicating the former to be more efficient.



中文翻译:

印度Odisha Sands Complex钛铁矿-焦炭复合颗粒的还原行为

目前,印度Chhatrapur的Odisha Sands Complex的钛铁矿精矿用于生产TiO 2通过在电弧炉中直接冶炼产生炉渣。但是,该方法涉及消耗过多的电能,并且由于起泡作用而难以处理电弧炉。在本说明书中已经提出了在冶炼之前预还原钛铁矿的更有效方法。特别地,已经对钛铁矿-焦炭复合颗粒的还原过程进行了研究。已经建立了钛铁矿原料和钛铁矿-焦炭复合颗粒还原性能的差异,并将其与预氧化的原料颗粒进行了比较。研究了各种工艺参数(如温度,停留时间和还原剂百分比)对静态床中复合颗粒金属化的影响。使用4 %%的焦炭成分,在1250°C下进行了约360分钟的还原,可实现约90%的金属化。此外,已通过化学分析,光学显微镜,场发射扫描电子显微镜和X射线衍射分析表征了还原的颗粒。还发现复合粒料的还原行为比预氧化粒料的还原行为更好,表明前者更有效。

更新日期:2020-07-16
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