Abstract

An efficient, fast, and straightforward procedure for the synthesis of arylazoxy sulfides can be achieved by coupling reaction between aryl nitrasocompounds and tribenzenesulphenamide under microwave irradiation. Using the present method, different kinds of aryl nitrasocompounds containing various dioxolane rings and various tribenzenesulphenamide derivatives were rapidly converted to the corresponding arylazoxy sulfides in good yield and short reaction time. The use of non-toxic solvent, simple and clean work-up, short reaction times and good yields are the advantages of this method.

Graphic abstract

中文翻译：

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微波辅助快速合成芳基偶氮硫化物

摘要

芳基硝杂化合物与三苯磺酰胺在微波辐射下的偶联反应可以实现合成芳基氮杂氧基硫化物的有效，快速和简单的方法。使用本发明的方法，含有各种二氧戊环和各种三苯磺酰胺衍生物的不同种类的芳基硝基化合物被快速转化为相应的芳基氮氧基硫化物。该方法的优点是使用无毒溶剂，后处理简单，清洁，反应时间短和产率高。

图形摘要