当前位置: X-MOL 学术Silicon › 论文详情
Our official English website, www.x-mol.net, welcomes your feedback! (Note: you will need to create a separate account there.)
High-Temperature Stability of Titanium Boride Reinforced Alumina-Silicon Carbide Based Composite
Silicon ( IF 3.4 ) Pub Date : 2020-06-06 , DOI: 10.1007/s12633-020-00498-y
Tamilselvam Nallusamy , Vijayakumar S

Alumina and Silicon Carbide based composites are routinely used in mechanical, automobile, ceramic and aerospace industries with numerous reinforcements. Reinforcements increase the physical, chemical, mechanical, thermal and tribological properties and make Al2O3-SiC suitable for a specific application. In this research, Titanium Boride powder of average size 95 nm reinforced into Al2O3-SiC nano-composite to enhance the thermal stability. The Al2O3-SiC nano-composite with 5, 10, 15 and 20 vol.% TiB2 were fabricated through pressureless sintering under an argon atmosphere at 1600 °C. The high-temperature thermal stability of Al2O3-SiC-TiB2 nano-composite was analyzed through the thermo-gravimetric analyzer (TG/DTA) with a warming rate of 10 °C/min and compared with Al2O3-SiC. A strong endothermic peak recorded at 1288 °C and excellent thermal stability recorded up to 1488 °C. 20% Titanium Boride added Alumina-Silicon Carbide nano-composite exhibited 6% reduced mass change and 20% increase in thermal stability at 1488 °C. The microstructure of the Al2O3-SiC-20 vol.% TiB2 was studied using XRD and SEM equipped with an EDX analysis facility. The SEM image displayed the surface morphology of the composite and XRD, EDX analysis exhibited the presence of Titanium particles with an average size of 95 nm.



中文翻译:

硼化钛增强氧化铝-碳化硅基复合材料的高温稳定性

氧化铝和碳化硅基复合材料通常用于机械,汽车,陶瓷和航空航天工业中,具有多种增强剂。增强增强了物理,化学,机械,热和摩擦学性能,并使Al 2 O 3 -SiC适合于特定应用。在这项研究中,将平均尺寸为95 nm的硼化钛粉末增强到Al 2 O 3 -SiC纳米复合材料中以增强热稳定性。通过在氩气氛下在1600℃下进行无压烧结来制备具有5、10、15、15和20vol。%的TiB 2的Al 2 O 3 -SiC纳米复合材料。Al 2 O的高温热稳定性通过热重分析仪(TG / DTA)以10℃/ min的升温速率分析3 -SiC-TiB 2纳米复合材料,并与Al 2 O 3 -SiC进行比较。在1288°C时记录到很强的吸热峰,在1488°C时记录到出色的热稳定性。添加的20%硼化钛氧化铝-碳化硅纳米复合材料在1488°C下的质量变化降低了6%,热稳定性提高了20%。Al 2 O 3 -SiC-20 vol。%TiB 2的微观结构使用配备有EDX分析设备的XRD和SEM对样品进行了研究。SEM图像显示了复合物的表面形态和XRD,EDX分析显示存在平均粒径为95nm的钛颗粒。

更新日期:2020-06-06
down
wechat
bug