Flow chemistry devices have seen an increase as research tools in recent years. We present a modular system for benchtop continuous flow that allows user flexibility and reliability in the pursuit of challenging chemistry. An oscillating baffle reactor mold-formed in perfluoroalkoxy alkane enables handling reactions forming solids. A LabView control system with help from Omega temperature controllers allows for simple and precise regulation of reaction conditions with real-time monitoring of the temperature and pressure. A new pressurized sample collection vessel allows for inert and pressurized sampling into multiple vials. An array of case studies serves to validate the system by demonstrating the use of interchangeable reactors with in-line heating and cooling, along with the ability to handle highly corrosive and reactive chemical reagents such as white fuming HNO₃.

中文翻译：

---

多功能模块化流动化学台式系统的开发

近年来，流化学设备已成为研究工具。我们提出了台式连续流的模块化系统，该系统允许用户在追求具有挑战性的化学过程中具有灵活性和可靠性。在全氟烷氧基烷烃中成型的振荡挡板反应器能够处理形成固体的反应。借助Omega温度控制器的LabView控制系统，可以通过实时监控温度和压力来简单，精确地调节反应条件。新的加压样品收集容器可将惰性样品和加压样品分成多个样品瓶。一系列案例研究通过演示可互换反应器与在线加热和冷却的结合来验证系统，₃。