Abstract A microwave absorber of MoS2-PANI with three-dimensional spherical structure was synthesized. The absorber was prepared by one-step hydrothermal strategy of a two-dimensional nanoflower-like MoS2 and in-situ oxidation polymerization reaction with an aniline monomer under ice bath conditions. It can be clearly seen from the SEM characterization that the structure of this three-dimensional MoS2-PANI microwave absorber is composed of a soft flower-like MoS2 as a carrier and a successful intercalation of two-dimensional nano-rod PANI. The effects of aniline monomer, initiator and molybdenum disulfide on the microwave absorption properties of MoS2-PANI nanocomposites were investigated by adjusting different mass ratios. The results show that the optimized reflection loss (RL) of the MoS2-PANI nanocomposites after interlayer is −59.78 dB, a matching thickness of 3.44 mm and an effective absorption frequency range of 6.56–9.68 GHz (RL

中文翻译：

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具有先进微波吸收性能的嵌入式 MoS2-PANI 纳米复合材料

摘要 合成了具有三维球形结构的MoS2-PANI微波吸收剂。该吸收剂是通过二维纳米花状二硫化钼和苯胺单体在冰浴条件下的原位氧化聚合反应的一步水热策略制备的。从SEM表征可以清楚地看出，这种三维MoS2-PANI微波吸收体的结构是由柔软的花状MoS2作为载体和二维纳米棒PANI的成功插层组成。通过调节不同的质量比，研究了苯胺单体、引发剂和二硫化钼对MoS2-PANI纳米复合材料微波吸收性能的影响。结果表明，夹层后MoS2-PANI纳米复合材料的优化反射损耗（RL）为-59.78 dB，