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Properties of C/C‐SiC composites produced via transfer moulding and inner siliconization
International Journal of Applied Ceramic Technology ( IF 2.1 ) Pub Date : 2020-05-28 , DOI: 10.1111/ijac.13548
Husam Ahmad 1 , Jonas Stiller 2 , Erik Päßler 2 , Daisy Nestler 2 , Lothar Kroll 2 , Guntram Wagner 1
Affiliation  

Short carbon fiber reinforced polymers (CFRP) are successfully prepared by transfer moulding technology. For this purpose, compounds on the basis of novolac/urotropin with different 6 mm chopped carbon fibers and silicon powder contents are produced utilizing a laboratory tempered sigma‐blade kneader. These compounds are then shaped into 46 × 8 × 3 mm3 CFRP specimens using a transfer moulding machine. Depending on the material composition, the conversion to C/C‐SiC composites is performed through liquid silicon infiltration (LSI) process or inner siliconization. First, the short fiber content is varied between 30 and 50 wt% and its influence on the process and properties of the composites is studied. Second, an investigation of the inner siliconization through the co‐mixing of silicon powder (1‐23 wt% in CFRPs) during the compound production as well as a comparison with the external silicon infiltration process are presented and discussed. According to the results, the best mechanical properties are achieved at a fiber content of 40 wt% in the case of the external silicon infiltration and at silicon content below 14 wt% for composites produced by the inner siliconization process.

中文翻译:

通过传递模塑和内部硅化生产的C / C-SiC复合材料的性能

短碳纤维增强聚合物(CFRP)通过传递模塑技术成功制备。为此,使用实验室回火的sigma-blade捏合机生产基于酚醛清漆/尿钙蛋白的化合物(具有不同的6毫米短切碳纤维和硅粉含量)。然后将这些化合物成型为46×8×3 mm 3CFRP样品使用传递模塑机。根据材料成分的不同,可以通过液态硅渗透(LSI)工艺或内部硅化工艺完成向C / C-SiC复合材料的转化。首先,短纤维含量在30至50 wt%之间变化,并研究了其对复合材料的工艺和性能的影响。其次,介绍并讨论了在化合物生产过程中通过共混硅粉(在CFRP中为1-23 wt%)进行内部硅化的研究,并与外部硅渗透过程进行了比较。根据结果​​,对于通过内部硅化工艺生产的复合材料,在外部硅渗透的情况下,纤维含量为40 wt%,在硅含量低于14 wt%时,可获得最佳的机械性能。
更新日期:2020-05-28
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