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The observation of tin islands in Nb3Sn thin films deposited by magnetron sputtering
Physica C: Superconductivity and its Applications ( IF 1.7 ) Pub Date : 2020-05-11 , DOI: 10.1016/j.physc.2020.1353667
Weiwei Tan , Rui Ma , Hui Pan , Huijing Zhao , Xin He , Xiaohuan Chen , Cuina Zhao , Xiangyang Lu

Superconducting Nb3Sn thin films have been produced on copper substrate by dc magnetron co-sputtering technique successfully. XRD and magnetic moment measurement demonstrate the exist of Nb3Sn crystal. By changing the ratio between niobium target sputtering current to tin target, the tin concentration in different films is varied. However, the experiment results indicate critical temperature TC of different Nb3Sn thin film are nearly invariable while the composition of Nb-Sn of those are changed. Highest TC of those films annealing at 650°C are around 12K, while 750°C annealing increase it to 15K. The SEM and element analysis results manifest inhomogenous distribution of tin atoms, where some tin islands appear over the film. The exist of tin-rich areas like tin islands is responsible for such particular performance of Nb3Sn films.



中文翻译:

磁控溅射沉积Nb 3 Sn薄膜中锡岛的观察

采用直流磁控共溅射技术在铜基片上成功制备了超导Nb 3 Sn薄膜。XRD和磁矩测量证明了Nb 3 Sn晶体的存在。通过改变铌靶溅射电流与锡靶之间的比率,可以改变不同膜中的锡浓度。然而,实验结果表明,不同的Nb 3 Sn薄膜的临界温度T C几乎不变,而Nb 3 Sn薄膜的组成却发生了变化。最牛逼Ç在650°C退火的那些薄膜中,约有12K,而在750°C退火则增加到15K。SEM和元素分析结果表明锡原子分布不均匀,在薄膜上出现了一些锡岛。Nb 3 Sn薄膜的这种特殊性能是造成锡岛等富锡区域的原因。

更新日期:2020-05-11
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