Abstract

The possibility of electrochemical synthesis of nanocomposites and nanocomposite films at pure-iron and steel electrodes using a 1-vinylimidazole–acrylic-acid co-polymer in the presence of chitosan is shown. Using UV- and IR-spectroscopy, XRD- and elemental analyses, the nanocomposite’s structure and composition were elucidated. The nanocomposite solubility was shown to be determined by intramolecular interaction of macromolecules in the 1-vinylimidazole–acrylic-acid co-polymer with gold nanoparticles. The nanocomposite thermal decomposition is a multistage process.

中文翻译：

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1-Vinylimidazole和丙烯酸基于金属的纳米复合材料的电合成

摘要

显示了在壳聚糖存在下使用1-乙烯基咪唑-丙烯酸共聚物在纯铁和钢电极上电化学合成纳米复合材料和纳米复合膜的可能性。使用紫外和红外光谱，XRD和元素分析，阐明了纳米复合材料的结构和组成。纳米复合材料的溶解度表明是由1-乙烯基咪唑-丙烯酸共聚物与金纳米颗粒中大分子的分子内相互作用决定的。纳米复合材料的热分解是一个多阶段的过程。