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Investigation of severe plastic deformation effects on microstructure and mechanical properties of WS2/AZ91 magnesium metal matrix composites
Materials Science and Engineering: A ( IF 6.4 ) Pub Date : 2020-03-09 , DOI: 10.1016/j.msea.2020.139211
Aqeel Abbas , Song-Jeng Huang

AZ91 reinforced with four different concentrations (0,0.3,0.6,1)wt% of WS2 micro particles were fabricated using stir casting method. The samples were deformed by equal channel angular pressing (ECAP) after homogenization. The scanning electron microscopy and X-ray diffraction were used to investigate the microstructure and phase composition respectively. The results reveal that rod-like precipitates produced during the homogenization process are refined and bounded in the grain boundaries by the combined effect of WS2 enrichment and increasing number of passes of ECAP. The needle precipitates are eminent in 1pass 0.3 wt%WS2/AZ91. The β-Mg17Al12 and extracted Al particles are dissolved and secondary phases are produced by dynamic recrystallization after 2pass 1 wt%WS2/AZ91. The maximum crystallite size and microstrain distribution have been observed for 1pass 0.6 wt%WS2/AZ91. The mechanical properties investigation represents that 2pass 0.6 wt%WS2/AZ91 has optimal yield strength and ultimate tensile strength. The (22.143)%, (44.735)% and (92) % increment in yield strength, ultimate tensile strength and elongation have been observed in 2pass 1 wt%WS2/AZ91 compared with homogenized monolithic AZ91 alloy respectively. The maximum young's modulus (6696.218MPa) has been found for 1pass homogenized WS2/AZ91 and minimum (4108.165MPa) for homogenized 0.6 wt%WS2/AZ91. The ECAP deformed 1pass 0.3 wt%WS2/AZ91 exhibits the maximum strain hardening rate. The YTS, UTS, and elongation are (30.41) %, (47.6) % and (51.9)% increased after 2pass-0.6 wt%WS2/AZ91.



中文翻译:

严重塑性变形对WS2 / AZ91镁金属基复合材料组织和力学性能的影响

采用搅拌铸造法制备了四种浓度为(0,0.3,0.6,1)wt%的WS 2微粒增强的AZ91 。均质后,通过等通道角挤压(ECAP)使样品变形。用扫描电子显微镜和X射线衍射分别研究了显微组织和相组成。结果表明,在均质化过程中产生的棒状沉淀物通过WS 2富集和ECAP通过次数增加的联合作用而细化并限制在晶界内。针状沉淀物以1pass 0.3 wt%WS 2 / AZ91突出。的β-Mg系17的Al 12然后经过2wt%1 wt%WS 2 / AZ91的动态重结晶溶解提取的Al颗粒并产生第二相。对于1pass 0.6wt%WS 2 / AZ91,已经观察到最大的微晶尺寸和微应变分布。力学性能研究表明,2pass 0.6 wt%WS 2 / AZ91具有最佳屈服强度和极限拉伸强度。与均质的整体AZ91合金相比,在2pass 1 wt%WS 2 / AZ91中分别观察到屈服强度,极限抗拉强度和伸长率分别增加了(22.143)%,(44.735)%和(92)%。已发现1次均质WS2 / AZ91的最大杨氏模量(6696.218MPa),均质0.6 wt%WS 2的最小杨氏模量(4108.165MPa)/ AZ91。ECAP变形1pass 0.3 wt%WS 2 / AZ91表现出最大的应变硬化速率。2pass-0.6 wt%WS 2 / AZ91后,YTS,UTS和伸长率分别增加(30.41)%,(47.6)%和(51.9)%。

更新日期:2020-03-09
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