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High performance SERS substrates using high surface roughness gold nanosheets assembled by nanowires
Vibrational Spectroscopy ( IF 2.5 ) Pub Date : 2020-03-01 , DOI: 10.1016/j.vibspec.2020.103041
Dapeng Xu , Zixiong Wang , Song Zhang , Wei Yang , Jian Chen

Abstract Gold nanosheets were prepared by a solid-state ionics method under a direct current electric field (DCEF) using fast ionic conductor Rb4Cu16Cl13I7 films. The morphology and chemical composition of the gold nanosheets were characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM) and energy dispersive spectrometer (EDS), respectively. Raman enhancement performance of the gold nanosheet substrates was detected by Rhodamine 6G (R6G) aqueous solutions as probe molecules. Gold nanosheets assembled by long-range order and short-range order pure gold nanowires and the nanowires were bamboo-shaped, the diameters of nanowires ranged from 30 to 70 nm. The limiting concentrations of R6G for the prepared gold nanosheet SERS substrates is 10−16 mol/L.

中文翻译:

使用由纳米线组装的高表面粗糙度金纳米片的高性能 SERS 基板

摘要 使用快离子导体 Rb4Cu16Cl13I7 薄膜在直流电场 (DCEF) 下通过固态离子法制备了金纳米片。金纳米片的形貌和化学成分分别通过扫描电子显微镜 (SEM)、透射电子显微镜 (TEM) 和能谱仪 (EDS) 进行表征。金纳米片基底的拉曼增强性能通过罗丹明 6G (R6G) 水溶液作为探针分子进行检测。由长程有序和短程有序纯金纳米线组装而成的金纳米片,纳米线呈竹节状,纳米线的直径为30~70 nm。制备的金纳米片 SERS 基底的 R6G 极限浓度为 10-16 mol/L。
更新日期:2020-03-01
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