The influence of essential process parameters on the adjustability of specific process and particulate properties of aluminum‐doped zinc oxide (AZO) nanocrystals during synthesis via the benzylamine route at low reaction kinetics is demonstrated by enabling time‐resolved access of the selected measurement technique. It is shown that the validity of the pseudo‐first‐order process kinetics could be extended to the minimum operable reaction kinetics. On the other hand, the impacts of the process temperature and the initial precursor concentration on both the process kinetics and the particle morphology are discussed. The obtained data provide a versatile tool for precise process control by adjusting defined application‐specific particle properties of AZO during synthesis.

中文翻译：

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通过苄胺途径在低反应动力学下形成铝掺杂氧化锌纳米晶体

通过在低反应动力学下通过苄胺途径合成铝掺杂氧化锌 (AZO) 纳米晶体的特定工艺和颗粒性质的可调节性，基本工艺参数的影响通过启用所选测量技术的时间分辨访问来证明。结果表明，准一级过程动力学的有效性可以扩展到最小可操作反应动力学。另一方面，讨论了工艺温度和初始前体浓度对工艺动力学和颗粒形态的影响。获得的数据通过在合成过程中调整定义的 AZO 特定应用颗粒特性，为精确过程控制提供了一种通用工具。