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Microscopic study of zinc nanoparticles synthesised using thermosetting polymer
Applied Microscopy Pub Date : 2019-12-01 , DOI: 10.1186/s42649-019-0018-0
Giriraj Tailor , Jyoti Chaudhay , Deepshikha Verma , Bhupendra Kr. Sarma

The present study reports the novel synthesis of Zinc nanoparticles (Zn NPs) by thermal decomposition method and its characterisation by Scanning Electron Microscope (SEM), Transmission Electron Microscope (TEM), and X-ray Diffraction Measurements (XRD). Synthesis of Zn NPs was achieved by using thermosetting polymer and zinc salts as precursor. Zn NPs were obtained on calcination at 850 °C for 30 min. SEM study reveals that synthesized nanoparticles are spherical in shape. XRD analysis shows that the Zn NPs formed are low crystalline in nature.

中文翻译:

热固性聚合物合成锌纳米粒子的显微研究

本研究报告了通过热分解法合成锌纳米粒子 (Zn NPs) 的新方法,并通过扫描电子显微镜 (SEM)、透射电子显微镜 (TEM) 和 X 射线衍射测量 (XRD) 对其进行表征。Zn NPs 的合成是通过使用热固性聚合物和锌盐作为前体来实现的。Zn NPs 是在 850 °C 下煅烧 30 分钟获得的。SEM 研究表明合成的纳米粒子是球形的。XRD 分析表明,形成的 Zn NPs 本质上是低结晶的。
更新日期:2019-12-01
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