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LR‐selHSQMBC: Simultaneous Detection and Quantification of Very Weak Long‐Range Heteronuclear NMR Correlations
ChemPhysChem ( IF 2.9 ) Pub Date : 2020-01-22 , DOI: 10.1002/cphc.201901142
Kumar Motiram‐Corral 1 , Alexandre A. Souza 2 , Josep Saurí 3 , Pau Nolis 1 , Teodor Parella 1
Affiliation  

The optimum detection and accurate measurement of longer‐range (4J and higher) heteronuclear NMR correlations is described. The magnitude and/or the sign of a wide range of large and small long‐range couplings can be simultaneously determined for protonated and non‐protonated 13C and 15N nuclei using the LR‐selHSQMBC experiment.

中文翻译:

LR-selHSQMBC:同时检测和定量非常弱的长距离异核核磁共振相关

描述了更长距离(4 J和更高)的异核NMR相关性的最佳检测和准确测量。可以使用LR-selHSQMBC实验同时确定质子化和非质子化的13 C和15 N核的大小和/或大范围和小范围远程耦合的范围。
更新日期:2020-01-22
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