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Influence of particulate morphology on microstructure and tribological properties of cold sprayed A380/Al2O3 composite coatings
Journal of Materials Science & Technology ( IF 10.9 ) Pub Date : 2020-01-08 , DOI: 10.1016/j.jmst.2020.01.028
Xiang Qiu , Naeem ul Haq Tariq , Lu Qi , Jun-Rong Tang , Xin-Yu Cui , Hao Du , Ji-Qiang Wang , Tian-Ying Xiong

In this study, three kinds of A380/Al2O3 composite coatings were prepared by cold spray (CS) using spherical, irregular and spherical + irregular shaped Al2O3 particulates separately mixed in the original A380 alloy powders. The influence of Al2O3 particulates’ morphology on the microstructural characteristics (i.e. retention of Al2O3 content in coatings, coating/matrix interfacial bonding, pore size distribution and morphology etc.) and wear performance of the coatings was investigated by scanning electron microscopy (SEM), X-ray computed tomography (XCT) and 3-D optical profilometry. Results indicated that the spherical Al2O3 shows obvious tamping effect during deposition process. As a result, the interface showed a wavy shape while the matrix and particulates were mechanical interlocked with much improved adhesion. In addition, the porosity of the coating was minimized and the pores exhibited curved spherical structure with reduced dimensions. The irregular Al2O3 particles predominantly displayed the embedding effect together with fragmentation of Al2O3 particulates. Consequently, poor coating/ matrix interfacial bonding, high porosity and the formation of angular-shaped pores were resulted in the coating. Dry sliding wear tests results revealed that the wear resistance of the coating is directly related with the retained content of Al2O3 in the coating. The coating containing irregular Al2O3 particulates displayed superior wear performance with its wear rate one seventh of that of the pure A380 alloy coating. The coating containing both kinds of Al2O3 particulates showed mixed characteristics of above two kinds of Al2O3 composite coatings.



中文翻译:

颗粒形态对冷喷涂A380 / Al 2 O 3复合涂层的组织和摩擦学性能的影响

在这项研究中,通过冷喷涂(CS)使用分别混合在原始A380合金粉末中的球形,不规则形状和球形+不规则形状的Al 2 O 3颗粒,通过冷喷涂(CS)制备了三种A380 / Al 2 O 3复合涂层。通过扫描研究了Al 2 O 3颗粒形态对显微组织特征(即涂层中Al 2 O 3的保留率,涂层/基体界面结合,孔径分布和形态等)和涂层磨损性能的影响。电子显微镜(SEM),X射线计算机断层扫描(XCT)和3-D光学轮廓仪。结果表明球形Al2 O 3在沉积过程中显示出明显的夯实效果。结果,界面呈波浪形,而基体和颗粒机械互锁,附着力大大提高。另外,涂层的孔隙率被最小化并且孔表现出尺寸减小的弯曲球形结构。不规则的Al 2 O 3颗粒主要表现出嵌入效果以及Al 2 O 3的碎裂微粒。结果,导致涂层中差的涂层/基体界面结合,高孔隙率和形成角形孔。干滑动磨损测试结果表明,涂​​层的耐磨性与涂层中Al 2 O 3的保留含量直接相关。含有不规则Al 2 O 3颗粒的涂层具有优异的磨损性能,其磨损率是纯A380合金涂层的七分之一。包含两种Al 2 O 3颗粒的涂层表现出上述两种Al 2 O 3复合涂层的混合特性。

更新日期:2020-01-08
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