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Silver-NPs functionalized hexagonal SBA-15 and lamellar SiO 2 -L81 mesoporous silica, synthesis and structural characterization
Journal of Sol-Gel Science and Technology ( IF 2.5 ) Pub Date : 2019-10-04 , DOI: 10.1007/s10971-019-05128-7
Issa M. El-Nahhal , Jamil K. Salem , Ahmed Al-agha

Abstract

Silver supported hexagonal SBA-15 and lamellar SiO2-L81 mesoporous silica were prepared via impregnation or co-condensation methods. FTIR, UV-vis., XRD, SEM, and TEM were utilized for determination of their structural properties of the Ag/SiO2 wasnanocomposites. The analysis confirmed that Ag-NPs were successfully loaded into/onto mesoporous silica (hexagonal SBA-15 and lamellar SiO2-L81). The loading of Ag-NPs showed a distortion of mesoporous silica structure via impregnation method, whereas it did not alter the mesoporosity structure, when the co-condensation method was used.



中文翻译:

银纳米粒子功能化的六角形SBA-15和层状SiO 2 -L81介孔二氧化硅,合成和结构表征

摘要

通过浸渍或共缩合方法制备了载银的六角形SBA-15和层状SiO 2 -L81介孔二氧化硅。FTIR,UV-vis。,XRD,SEM和TEM用于测定Ag / SiO 2纳米复合材料的结构性能。分析证实Ag-NPs成功地加载到介孔二氧化硅中(六角形SBA-15和层状SiO 2 -L81)。Ag-NPs的负载量通过浸渍法显示出介孔二氧化硅结构的变形,而当使用共缩合方法时,它并没有改变介孔结构。

更新日期:2020-01-16
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