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Combination of (13)C-(13)C COSY and DARR (COCODARR) in solid-state NMR.
Solid State Nuclear Magnetic Resonance ( IF 3.2 ) Pub Date : 2008-07-19 , DOI: 10.1016/j.ssnmr.2008.05.001
Masashi Fukuchi 1 , K Takegoshi
Affiliation  

In this work, we describe a new 2D (13)C-(13)C correlation experiment in solids, in which (13)C-(13)C J-correlation (COSY) and dipolar correlation (DARR) are recorded at the same time. The sequence is similar to COCONOSY in the liquid-state NMR, in which (1)H-(1)H COSY and NOESY spectra are obtained in a single experiment. The combined COSY and DARR experiment facilitates assignment of (13)C signals in solids.

中文翻译:

固态NMR中(13)C-(13)C COZY和DARR(COCODARR)的组合。

在这项工作中,我们描述了一个新的固体二维(13)C-(13)C相关实验,其中在(13)C-(13)C J相关(COSY)和偶极相关(DARR)记录在固体中。同时。该序列类似于液相NMR中的COCONOSY,其中在单个实验中获得(1)H-(1)H COZY和NOESY光谱。COZY和DARR的组合实验有助于固体中(13)C信号的分配。
更新日期:2019-11-01
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