Molybdenum disulfide (MoS₂), as a significant microwave absorption materials, has been widely reported. However, it is unclear and insufficient about its microwave absorption mechanism. In this work, a series of MoS₂-based materials with different morphology, including MoS₂ nanosheets (MoS₂-NS), hierarchical MoS₂ (H-MoS₂) microspheres, hollow hierarchical MoS₂ (HH-MoS₂) microspheres and hydrangea-like MoS₂/C (MoS₂/C) microspheres, were synthesized via hydrothermal reaction. More importantly, the microwave absorption mechanism and the dielectric properties as well as microwave absorption performance (MAP) were systemically studied. The results indicated that MoS₂/C exhibited eminent dielectric properties and MAP, which resulted from the unique structure and component. The minimum reflection loss (RL) value of MoS₂/C microspheres/wax with 30 wt% loading is −44.67 dB at the thickness of 1.4 mm, and the corresponding bandwidth with effective attenuation (RL < -10 dB) is up to 3.32 GHz (11.7–15.02 GHz).

已经广泛报道了作为重要的微波吸收材料的二硫化钼（MoS ₂）。但是，其微波吸收机理尚不清楚且不足。在这项工作中，一系列具有不同形态的基于MoS ₂的材料，包括MoS ₂纳米片（MoS ₂ -NS），分层MoS ₂（H-MoS ₂）微球，空心分层MoS ₂（HH-MoS ₂）微球和像绣球的MoS ₂ / C（MoS ₂ /C）通过水热反应合成微球。更重要的是，系统地研究了微波吸收机理，介电性能以及微波吸收性能（MAP）。结果表明，MoS ₂ / C表现出优异的介电性能和MAP，这是由于其独特的结构和成分所致。负载为30 wt％的MoS ₂ / C微球/蜡的最小反射损耗（RL）值在1.4毫米厚度下为−44.67 dB，并且具有有效衰减（RL <-10 dB）的相应带宽最高为3.32 GHz（11.7–15.02 GHz）。