This experiment prepares a large (M_r: 1821 g mol^–1) triple helicate complex quickly in one pot from inexpensive starting materials. The protocol illustrates the power of self-assembly in a simple manner that is suitable for second-year general chemistry students using reversible imine bond and metal–ligand bond formation. Plastic molecular models and ¹H NMR spectroscopy are used to elucidate the structure of the self-assembled product.

中文翻译：

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快速而直接的超分子自组装实验，以制备和表征三螺旋复合物。

该实验中准备一个大的（中号_[R：1821克摩尔^-1）三重helicate在从廉价的原料一锅复杂快。该协议以简单的方式说明了自组装的能力，适用于使用可逆亚胺键和金属-配体键形成的二年级一般化学专业的学生。使用塑料分子模型和¹ H NMR光谱来阐明自组装产品的结构。