Journal of the European Ceramic Society ( IF 5.7 ) Pub Date : 2018-01-31 , DOI: 10.1016/j.jeurceramsoc.2018.01.024 Federica Bezzi , Federica Burgio , Paride Fabbri , Selene Grilli , Giuseppe Magnani , Elena Salernitano , Matteo Scafè
In order to improve the oxidation resistance of Cf/Cs produced by chemical vapour infiltration, a multilayer coating based on silicon carbide and molybdenum disilicide was produced by two-step pack cementation technique. The inner SiC layer with a thickness up to 25 μm was obtained without promoted reaction additives by varying the composition, and thermal treatment conditions. The SiC/SiC-MoSi2 coating was produced with a thickness up to 80 μm by two step pack cementation, considering the effect of the inner layer characteristic. The enhancement of the oxidation resistance, observed in SiC/SiC-MoSi2 coated Cf/Cs by means of thermal analysis in flowing air up to 1500 °C, was due to the formation of SiO2 promoted by the passive oxidation of silicon carbide and molybdenum disilicide.
中文翻译:
通过两步填充胶结用于C f / C复合材料的SiC / MoSi 2基涂层
为了提高化学气相渗透法产生的C f / Cs的抗氧化性,通过两步填充胶结技术制备了基于碳化硅和二硅化钼的多层涂层。通过改变组成和热处理条件,可以获得厚度不超过25μm的内部SiC层,而没有促进反应的添加剂。考虑到内层特性的影响,通过两步填充胶结生产了厚度最大为80μm的SiC / SiC-MoSi 2涂层。在高达1500°C的流动空气中,通过热分析在SiC / SiC-MoSi 2涂层的C f / Cs中观察到的抗氧化性增强是由于SiO 2的形成 由碳化硅和二硅化钼的被动氧化促进。