Abstract

Acrylohydroxamic acid, which is a useful monomer for the preparation of polymeric materials, has been prepared in a straightforward, two-step synthesis from readily available starting materials. The key steps are coupling of acrylic acid with O-tetrahydropyranylhydroxyl amine to provide protection of the hydroxylamine functionality, followed by acid cleavage of the protecting group.

Acrylohydroxamic acid, which is a useful monomer for the preparation of polymeric materials, has been prepared in a straightforward, two-step synthesis from readily available starting materials. The key steps are coupling of acrylic acid with O-tetrahydropyranylhydroxyl amine to provide protection of the hydroxylamine functionality, followed by acid cleavage of the protecting group.

中文翻译：

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实用的克级异羟肟酸的合成

摘要

丙烯酸异羟肟酸是制备聚合物材料的有用单体，它是从容易获得的起始原料中以直接，两步合成的方式制备的。关键步骤是将丙烯酸与O-四氢吡喃基羟胺偶联以提供羟胺官能度的保护，然后将保护基进行酸裂解。

丙烯酸异羟肟酸是制备聚合物材料的有用单体，它是从容易获得的起始原料中以直接，两步合成的方式制备的。关键步骤是将丙烯酸与O-四氢吡喃基羟胺偶联以提供羟胺官能度的保护，然后将保护基进行酸裂解。