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Determination of the length and diameter of nanorods by a combination of analytical ultracentrifugation and scanning mobility particle sizer†
Nanoscale Horizons ( IF 9.7 ) Pub Date : 2017-06-06 00:00:00 , DOI: 10.1039/c7nh00050b
T. Thajudeen 1, 2, 3, 4, 5 , J. Walter 1, 2, 3, 4, 5 , R. Srikantharajah 1, 2, 3, 4 , C. Lübbert 1, 2, 3, 4, 5 , W. Peukert 1, 2, 3, 4, 5
Affiliation  

A combination of orthogonal measurement techniques is utilized in this study to predict the average lengths and diameters of colloidal nanorods. Sedimentation coefficient distributions and electrical mobility distributions obtained from analytical ultracentrifugation and a scanning mobility particle sizer, respectively, are used for the hydrodynamic correlation. The method is validated theoretically and application to Au and ZnO nanorod samples is shown. The results demonstrate that the combination of both measurement techniques is an excellent method for the two-dimensional characterization of nanorods.

中文翻译:

分析超离心和扫描迁移率粒度仪的组合测定纳米棒的长度和直径

在这项研究中使用正交测量技术的组合来预测胶体纳米棒的平均长度和直径。分别由分析超离心和扫描迁移率粒度仪获得的沉降系数分布和电迁移率分布用于流体动力学相关性。该方法在理论上得到了验证,并显示了其在Au和ZnO纳米棒样品中的应用。结果表明,两种测量技术的结合是纳米棒二维表征的极好方法。
更新日期:2017-06-06
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