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Palladium-Catalyzed Weak Chelation-Assisted Site-Selective C–H Arylation of N-Aryl Pyridones via 2-fold C–H Activation J. Org. Chem. (IF 3.6) Pub Date : 2024-04-17 Maniya V. Nanjegowda, Shubhajit Basak, Tripti Paul, Tharmalingam Punniyamurthy
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Stable 2-Azaallyl Salts as a Bridge between 2H-Azirines and Densely Functionalized 2H-Pyrroles J. Org. Chem. (IF 3.6) Pub Date : 2024-04-17 Julia I. Pavlenko, Anastasiya V. Agafonova, Pavel A. Sakharov, Ilia A. Smetanin, Alexander F. Khlebnikov, Mariya A. Kryukova, Mikhail S. Novikov
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Revisiting Hafner’s Azapentalenes: The Chemistry of 1,3-Bis(dimethylamino)-2-azapentalene J. Org. Chem. (IF 3.6) Pub Date : 2024-04-17 Enikő Meiszter, Tamás Gazdag, Péter J. Mayer, Attila Kunfi, Tamás Holczbauer, Máté Sulyok-Eiler, Gábor London
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Precise Synthesis of Diastereomers of Spiro-oxindole Derivatives through Dynamic Covalent Transformation J. Org. Chem. (IF 3.6) Pub Date : 2024-04-17 Xiao-Qian Liu, Jian-Dong Zhang, Shun-Jun Ji, Xiao-Ping Xu
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Metal-Free Bisamidation of N-Tosylhydrazones with Carboxylic Acids Promoted by Tetrabutylammonium Iodide and tert-Butyl Hydroperoxide J. Org. Chem. (IF 3.6) Pub Date : 2024-04-17 Ali Shamnad, Kalinga H. Nayak, Beneesh P. Babu
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Total Synthesis and Cytotoxicity Evaluation of Pareitropone and Analogues J. Org. Chem. (IF 3.6) Pub Date : 2024-04-17 Hyeonjeong Kim, Nara Shin, Suk-Koo Hong, Jongbeom Park, Sangkil Nam, David A. Horne, J. R. Choi, Jin Kun Cha, Young Gyu Kim
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Electronic and Magnetic Interactions in 6-Oxoverdazyl Diradicals: Connection through N(1) vs C(3) Revisited J. Org. Chem. (IF 3.6) Pub Date : 2024-04-16 Agnieszka Bodzioch, Emilia Obijalska, Rafał Jakubowski, Małgorzata Celeda, Anita Gardias, Damian Trzybiński, Paweł Tokarz, Jacek Szczytko, Krzysztof Woźniak, Piotr Kaszyński
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Ruthenium(II)-Catalyzed Sequential C–H/N–H Alkene Annulation Cascade of Phenanthroimidazoles: Synthesis and Photophysical Studies J. Org. Chem. (IF 3.6) Pub Date : 2024-04-16 Rekha Thakur, Kamaldeep Paul
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Mechanism and Enantioselectivity in QUINOX-Catalyzed Asymmetric Allylations of Aromatic Aldehydes: Solvent and Substituent Effects J. Org. Chem. (IF 3.6) Pub Date : 2024-04-16 Pingli Lv, Rongxiu Zhu, Dongju Zhang, Steven E. Wheeler
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Gold-Catalyzed Reactions of Enynals with Alkenes for Synthesis Binaphthyl Derivatives J. Org. Chem. (IF 3.6) Pub Date : 2024-04-16 Jun-Jie Hao, Juan Wu, Tao Jiang, Hejiang Luo, Rong-Tao Li
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Synthesis of Acyl Cyclopentaquinolinones through Simultaneous Construction of the Heterocyclic Scaffold and Introduction of the Acyl Group J. Org. Chem. (IF 3.6) Pub Date : 2024-04-16 Lian Xue, Chang Gao, Xinying Zhang, Xuesen Fan
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TBHP/Et3N-Promoted Chemoselective Formylation and Peroxidation of Pyrrolo[2,1-a]isoquinolines J. Org. Chem. (IF 3.6) Pub Date : 2024-04-16 Xiang Huang, Jing Zhou, Shu-Chen Pei, Hai-Lei Cui
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Trivalent Phosphine-Catalyzed [4+1] Spiro-annulation Reaction Using Allenyl Imide and Methylene Cyclocompounds J. Org. Chem. (IF 3.6) Pub Date : 2024-04-16 Zi-Qiu Zhang, Zhen-Kai Zhang, Yu-Hao Wang, Bo-Ting Chen, Feng-Kai He, Yi-Long Wang, Tao Shu, Yi-Yong Huang
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Phosphoric Acid Catalyzed N-Addition/ C-Addition Reaction of 3-Vinyl Indoles with Pyrazole/Pyrazolone to Construct Pyrazole-Substituted 3-(1-Heteroarylethyl)-indole Scaffolds J. Org. Chem. (IF 3.6) Pub Date : 2024-04-15 Jie Luo, Ji-Xing Zhao, Tao He, Ping Liu, Chun-Tian Li
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Organocatalytic Asymmetric Conjugate Addition of Fluorooxindoles to Quinone Methides J. Org. Chem. (IF 3.6) Pub Date : 2024-04-15 Maria Bouda, Jeffery A. Bertke, Christian Wolf
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Non-Tertiary Alkyl Substituents Enhance High-Temperature Radical Trapping by Phenothiazine and Phenoxazine Antioxidants J. Org. Chem. (IF 3.6) Pub Date : 2024-04-15 Luke A. Farmer, Derek A. Pratt
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Template Synthesis of Disilacycloalkanes Utilizing the Reactivity of a Siloxane Bond J. Org. Chem. (IF 3.6) Pub Date : 2024-04-15 Yuyang Tu, Yusuke Inagaki, Wataru Setaka
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Visible-Light-Promoted Deoxygenative Alkylation of Quinoxalin-2(1H)-ones with Activated Alcohols J. Org. Chem. (IF 3.6) Pub Date : 2024-04-15 Lili Wang, Pengyuan Yang, Jinwei Yuan, Wei Lian, Xinrong Jin, Sanyu Zhang, Liangru Yang, Dongliang Xing
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Arylazopyrazoles for Conjugation by CuAAC Click Chemistry J. Org. Chem. (IF 3.6) Pub Date : 2024-04-15 Alisa-Maite Kauth, Rebecca Niebuhr, Bart Jan Ravoo
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Electrochemical Benzylic C(sp3)-H Imidation Enabled by Benzoic Acid Derived Radicals J. Org. Chem. (IF 3.6) Pub Date : 2024-04-15 Peng Qian, Dan Zhu, Xiaoli Wang, Qi Sun, Sheng Zhang
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Iodine-Catalyzed Diversity-Oriented Synthesis of 3,4-Heterocycle-Fused Coumarins from 4-Aminocoumarins and Aurones in Different Solvent J. Org. Chem. (IF 3.6) Pub Date : 2024-04-15 Xuequan Wang, Zhen Jiang, Chahui Du, Lin Ma, Dan Yue, Changhui Yang, Suyue Duan, Xianfu Shen
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TFA-Promoted Cascade Sulfonylation/Rearrangement/Cyclization of 1,5-Diynols and Sodium Sulfinates to Construct Sulfonylated Benzo[b]fluorenes J. Org. Chem. (IF 3.6) Pub Date : 2024-04-14 Shimin Jiang, Meng Liang, Jiang Bai, Ruchun Yang, Xi Chen, Haiyang Huang, Hai-Xin Ding, Mu-Jia Luo, Xian-Rong Song, Qiang Xiao
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Enzyme-Responsive Fluorescent Labeling Strategy for In Vivo Imaging of Gut Bacteria J. Org. Chem. (IF 3.6) Pub Date : 2024-04-12 Wenchao Lang, Dunji Shu, Songhan Liu, Caixia Sun, Huihong Liu, Qianqian Huang, Guojiang Mao, Sheng Yang, Bengang Xing
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Synthesis of Vicinal anti-Amino Alcohols from N-tert-Butanesulfinyl Aldimines and Cyclopropanols J. Org. Chem. (IF 3.6) Pub Date : 2024-04-13 Sandra Hernández-Ibáñez, Juan F. Ortuño, Ana Sirvent, Carmen Nájera, José Miguel Sansano, Miguel Yus, Francisco Foubelo
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Iodine(III)-Catalyzed Oxidative Cyclization of Aryl Amines to Construct N-Alkylbenzimidazoles J. Org. Chem. (IF 3.6) Pub Date : 2024-04-13 Carmen Margaret White, Sherlyn Cazares, Efren D. Gonzalez-Cortes, Tom G. Driver
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Synthesis of α,α-Difluoro-β-amino Ketones from N-Boc-α-Amidosulfones and Pentafluoro-gem-diols J. Org. Chem. (IF 3.6) Pub Date : 2024-04-12 Baharul Islam, Suresh P. Sulochana, David A. Colby
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Density Functional Theory Study on the Mechanism of Nickel-Catalyzed 3,3-Dialkynylation of 2-Aryl Acrylamides Via Double Vinylic C–H Bond Activation J. Org. Chem. (IF 3.6) Pub Date : 2024-04-12 Ailin Gao, Zhenfeng Shang, Ruifang Li, Xiufang Xu
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Enantioselective Total Synthesis of the Neurotoxin Caramboxin J. Org. Chem. (IF 3.6) Pub Date : 2024-04-12 Benoit Derrien, Karine Leblanc, Laurent Evanno, Emmanuelle Drège
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Catalysts-Controlled Roles Exchange between 2,3-Diaryl-2H-azirines and Acetone: Chemodivergent Synthesis of Pyrroles and 3-Oxazolines J. Org. Chem. (IF 3.6) Pub Date : 2024-04-11 Haipeng Hu, Yangu Liu, Beining Wang, Shangyi Fan, Rui Deng, Xiang Pu, Yu Huang
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Phenoxaphosphonium Mixed Ylides in Ring Expansion Reaction J. Org. Chem. (IF 3.6) Pub Date : 2024-04-12 Anton S. Nenashev, Dmitrii A. Dospekhov, Mikhail V. Zavaruev, Irina I. Levina, Vitaly A. Roznyatovsky, Andrey V. Mironov, Anna S. Pavlova, Tatyana A. Podrugina
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Light-Induced Generation and Cycloaddition Reactions of Benzyne: Synthesis of Naphthoxindoles E and Annulated Indolizines J. Org. Chem. (IF 3.6) Pub Date : 2024-04-12 Haya Khan, Dhiraj Barman, Subhabrata Sen
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Benchmarking Trisaminocyclopropeniums as Mediators for Anodic Oxidation Reactions J. Org. Chem. (IF 3.6) Pub Date : 2024-04-12 Sabrina N. Carneiro, Joshua D. Laffoon, Long Luo, Melanie S. Sanford
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One-Pot Three-Component Reaction for the Synthesis of 3,4-Dihydroquinazolines and Quinazolin-4(3H)-ones J. Org. Chem. (IF 3.6) Pub Date : 2024-04-12 Shiwei Chen, Yeong Shin Ji, Yuri Choi, So Won Youn
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Synthesis of Spiro Polycyclic N-Heterocycles and Indolecarbazoles via Merging Oxidative Coupling and Cascade Palladium-Catalyzed Intramolecular Oxidative Cyclization J. Org. Chem. (IF 3.6) Pub Date : 2024-04-12 Yu Dong, Mei-Feng Lan, Yue-Qin Lin, Lin Chen, Chun-Mei Wu, Zhi-Fan Wang, Zhi-Chuan Shi, Guo-wei Deng, Bing He
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Oxidative Cascade Iodocyclization of 1,n-Dienes: Synthesis of Iodinated Benzo[b]azepine and Benzo[b]azocine Derivatives J. Org. Chem. (IF 3.6) Pub Date : 2024-04-11 Pengpeng Tan, Shilong Wang, Guiling Li, Huichao Wang, Ziheng Zhao, Haochen Jiang, Lei Xie, Liru Yang, Jinchun Chen, Zhen Zhang
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A Three-Component Synthesis of Spiropyrrolines J. Org. Chem. (IF 3.6) Pub Date : 2024-04-11 Kanchanbala Sahoo, Nityaprakash Patra, Rambabu Dandela, Barla Thirupathi
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Extending the Scope of the C-Functionalization of Cyclam via Copper(I)-Catalyzed Alkyne–Azide Cycloaddition to Bifunctional Chelators of Interest J. Org. Chem. (IF 3.6) Pub Date : 2024-04-11 Cédric Ollier, Alejandro Méndez-Ardoy, Fernando Ortega-Caballero, José L. Jiménez-Blanco, Nathalie Le Bris, Raphaël Tripier
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Selected Electrosynthesis of 3-Aminopyrazoles from α,β-Alkynic Hydrazones and Secondary Amines J. Org. Chem. (IF 3.6) Pub Date : 2024-04-11 Dong Tang, Wei Zhang, Jingwen Ji, Rui Jiang, Yaya Wan, Wei Ma, Pengjuan Zhou
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Indium Promotes Direct Sulfonamidation of Unactivated Alcohols J. Org. Chem. (IF 3.6) Pub Date : 2024-04-11 Yaoyao Ban, Yuhan Liu, Shuwei Zhang, Xiaodong Jia, Pan Gao, Yu Yuan
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Accessing 1,8-Naphthyridone-3-carboxylic Acid Derivatives and Application to the Synthesis of Amfonelic Acid J. Org. Chem. (IF 3.6) Pub Date : 2024-04-11 Kaijuan Wang, Chengcheng Gong, Weiwei Xiao, Ablimit Abdukader, Dong Wang
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Domino Michael/Oxa-Michael Reactions of the Unsymmetric Double Michael Acceptor for Access to Bicyclic Furo[2,3-b]pyrrole J. Org. Chem. (IF 3.6) Pub Date : 2024-04-10 Hang Li, Ning Wang, Zhitin Zhou, Lipeng Long, Xun Li, Yiping Qian, Liang Qiao
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Readily Accessible and Brightly Fluorogenic BODIPY/NBD–Tetrazines via SNAr Reactions J. Org. Chem. (IF 3.6) Pub Date : 2024-04-10 Murat Işık, Mehmet Ali Kısaçam
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[Au]-Catalyzed Cyclization of Propargyl-Tethered Ene-Amides: Substrate-Dependent Access to Tetrasubstituted Pyrroles, Aminophenols, and Dihydropyridines J. Org. Chem. (IF 3.6) Pub Date : 2024-04-10 Suraj, K. C. Kumara Swamy
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Palladium-Catalyzed Iodine Assisted Carbonylation of Indoles with ClCF2CO2Na and Alcohols J. Org. Chem. (IF 3.6) Pub Date : 2024-04-10 Mengting Cao, Dandan Zuo, Dan Wang, Yafei Li, Jingjing Zhao, Jiajing Tan, Pan Li
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Synthesis of Quillaic Acid through Sustainable C–H Bond Activations J. Org. Chem. (IF 3.6) Pub Date : 2024-04-10 Yi-Chi Wang, Cheng-Ru Chen, Chien-Yi Chen, Pi-Hui Liang
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Diastereoselective Synthesis of Less Accessible Fluorine-Containing Acyclic Tetrasubstituted Stereocenters via Electrophilic Fluorination of β,β-Disubstituted Metalloenamines J. Org. Chem. (IF 3.6) Pub Date : 2024-04-10 Tao Liu, Nuermaimaiti Yisimayili, Li-Feng Chu, Chong-Dao Lu
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Total Synthesis of (±)-Oxacyclododecindione J. Org. Chem. (IF 3.6) Pub Date : 2024-04-10 Kevin Seipp, Vincent Grölz, Hagen Glass, Elisabeth Quraishi, Nina Vierengel, Till Opatz
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Total Syntheses of Discoipyrroles A, B, and C, Three Marine Natural Products J. Org. Chem. (IF 3.6) Pub Date : 2024-04-10 Gaurav G. Dake, Krishna P. Kaliappan
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The Development of a Sulfamate-Tethered Aza-Michael Cyclization Allows for the Preparation of (−)-Negamycin tert-Butyl Ester J. Org. Chem. (IF 3.6) Pub Date : 2024-04-10 Harshit Joshi, Appasaheb K. Nirpal, Debobrata Paul, Steven P. Kelley, Joel T. Mague, Shyam Sathyamoorthi
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Light-Driven Access to Selenium-Substituted Thiazole-2-imine Derivatives J. Org. Chem. (IF 3.6) Pub Date : 2024-04-09 Tangle Li, Dandan Hu, Yiwen Huang, Yu Zhou, Jun-Qi Zhang, Chun Zhang, Yili Zhang, Yanan Hou, Hongjun Ren
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Intramolecular 1,2-Aroyl Migration in Spiro Donor–Acceptor Cyclopropanes: Formation of 1,4-Naphthoquinones and 1-Naphthols as Ring-Expansion Products J. Org. Chem. (IF 3.6) Pub Date : 2024-04-09 Franklin Leslin Daniel, Kannupal Srinivasan
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Revealing the Mechanism of Alcohol Dehydroxylation and C–C Bond Formation through Concerted Catalysis by Ir/Cu Bimetallic Complexes J. Org. Chem. (IF 3.6) Pub Date : 2024-04-09 Taiming Bai, Hui Li
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Gold-Catalyzed Oxidation Reactions of Thioalkynes with Quinoline N-Oxides: A DFT Study J. Org. Chem. (IF 3.6) Pub Date : 2024-04-09 Wanying Zhang, Baoping Ling, Siwei Bi
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Molecular Iodine as a Catalyst for Alkene Difluorination J. Org. Chem. (IF 3.6) Pub Date : 2024-04-09 Tsugio Kitamura, Juzo Oyamada, Masahiro Higashi, Yosuke Kishikawa
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NBS-Promoted Synthesis of Thiocyanated Aminomaleimides and Site-Selective Intramolecular Cyclization Access to 1,4-Benzothiazepines via S–CN Bond Cleavage J. Org. Chem. (IF 3.6) Pub Date : 2024-04-09 Qi Yang, Shuntao Huang, Lu Yin, Zhuoyu Wang, Xuebing Chen, Chao Huang
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Impact of Solvent and Protonation State on Rotational Barriers in [s]-Triazines J. Org. Chem. (IF 3.6) Pub Date : 2024-04-09 Liam E. Claton, Hongjun Pan, Eric E. Simanek
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Pyramidalization of the Carboxamide sp2-Center in Peptide Structures J. Org. Chem. (IF 3.6) Pub Date : 2024-04-09 Henri Brunner, Masahiro Ikeshita, Takashi Tsuno
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MSTFA as an Effective TMS Source for the TMSOTf-Catalzyed Synthesis of Cyclic Acetals J. Org. Chem. (IF 3.6) Pub Date : 2024-04-09 Suttipol Radomkit, Jada A. H. White, Eugene Chong, Yongda Zhang
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Disproof of the Structures and Biosynthesis of Ergoynes, Gs-Polyyne–l-Ergothioneine Cycloadducts from Gynuella sunshinyii YC6258 J. Org. Chem. (IF 3.6) Pub Date : 2024-04-09 Daiki Kawahara, Kenji Kai
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Visible-Light-Driven Bifunctional Photocatalytic Radical-Cascade Selenocyanation/Cyclization of Acrylamides with KSeCN J. Org. Chem. (IF 3.6) Pub Date : 2024-04-09 Xinxin Ren, Tao Zhang, Bin Wang, Weiwei Jin, Yu Xia, Shaofeng Wu, Chenjiang Liu, Yonghong Zhang